• 专利标题:   Preparation of Prussian blue material for composite reduction of graphene oxide, used as battery anode material, involves reacting graphene oxide, sodium ferrocyanide, ascorbic acid, sodium citrate and hydrochloric acid.
  • 专利号:   CN108217630-A
  • 发明人:   WU J, JIN X, CUI Y, TANG Q
  • 专利权人:   HARBIN INST TECHNOLOGY SHENZHEN GRADUATE
  • 国际专利分类:   C01B032/184, C01G049/00, H01M010/054, H01M004/58
  • 专利详细信息:   CN108217630-A 29 Jun 2018 C01B-032/184 201852 Pages: 10 Chinese
  • 申请详细信息:   CN108217630-A CN11480277 29 Dec 2017
  • 优先权号:   CN11480277

▎ 摘  要

NOVELTY - The preparation of Prussian blue material, involves ultrasonically dispersing graphene oxide in aqueous solution of sodium ferrocyanide, adding ascorbic acid as antioxidants, adding sodium citrate to reduce reaction rate, adding hydrochloric acid to adjust solution to be acidic, heating and stirring under protection of inert gas, washing, vacuum drying and reducing obtained product by microwave irradiation. USE - Preparation of Prussian blue material for composite reduction of graphene oxide, used as battery anode material (claimed). ADVANTAGE - The method enables preparation of Prussian blue material with improved specific capacity by simple, quick and economical process.