• 专利标题:   Preparation of graphene involves mixing copper nitrate, glucose, and sodium chloride, dissolving mixture in water, spray-drying, calcining under protection of argon and hydrogen gas mixture, washing away sodium chloride, and drying.
  • 专利号:   CN108793130-A
  • 发明人:   LI J, HAN T, HE C, ZHAO N, SHI C, LIU E
  • 专利权人:   UNIV TIANJIN
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN108793130-A 13 Nov 2018 C01B-032/184 201901 Pages: 9 Chinese
  • 申请详细信息:   CN108793130-A CN10773758 15 Jul 2018
  • 优先权号:   CN10773758

▎ 摘  要

NOVELTY - Preparation of graphene comprises mixing copper nitrate, glucose, and sodium chloride at certain molar ratio; dissolving mixture in water; uniformly stirring; spray-drying at 130-180 degrees C to obtain precursor powder of self-assembled sodium chloride, glucose and copper nitrate for chemical deposition process; calcining precursor powder of self-assembled structure at 730-760 degrees C in tube furnace under 1:1 ratio of argon and hydrogen gas mixture for 2 hours; washing away sodium chloride; and drying to obtain surface-loaded copper particles of graphene structure. USE - Preparation of graphene. ADVANTAGE - The method has cheap and easy to obtain raw materials, and realizes mass production and loading of copper particles on surface of graphene.