• 专利标题:   Preparing cellulose/oxidized graphene carbon aerogel for heavy metal adsorption and waste water purification or electrode materials, involves dissolving sodium hydroxide and carbamide in water.
  • 专利号:   CN109019597-A
  • 发明人:   YANG F, TANG L, FENG Y, LI Y, HE W
  • 专利权人:   UNIV SOUTH CHINA TECHNOLOGY
  • 国际专利分类:   B01J020/20, B01J020/28, B01J020/30, C01B032/198, C01B032/318, C01B032/336, C01B032/348, C02F001/28, C02F101/20
  • 专利详细信息:   CN109019597-A 18 Dec 2018 C01B-032/348 201918 Pages: 7 Chinese
  • 申请详细信息:   CN109019597-A CN10782750 17 Jul 2018
  • 优先权号:   CN10782750

▎ 摘  要

NOVELTY - Preparing cellulose/oxidized graphene carbon aerogel involves dissolving sodium hydroxide and carbamide in water to obtain sodium hydroxide/urea aqueous solution as solvent, pre-cooling solvent obtained to (-)8-(-)15 degrees C, then absolute dry bleached flax pulp is added in amount of 1-5 wt.% with respect to mass of solvent, stirred and mixed uniformly to obtain cellulose solution. The graphene oxide is added into cellulose solution, stirred and dispersed uniformly, then heated to 40-60/oC to make gelatinized to obtain cellulose/oxidized graphene hydrogel, then freezed and dried to obtain cellulose/graphene oxide gel. The obtained cellulose/graphene oxide gel is subjected under vacuum condition for high temperature carbonization, and then acid etched, water washed, filtered, finally vacuum dried to obtain cellulose/oxidized graphite alkene carbon aerogel. The conditions for high temperature carbonization are low temperature pre-carbonizing at 180-220 degrees C for 1-3 hours. USE - Method for preparing cellulose/oxidized graphene carbon aerogel for heavy metal adsorption and waste water purification or electrode materials (claimed). ADVANTAGE - The method enables to prepare cellulose/oxidized graphene carbon aerogel that has good hydrophilicity and chemical modification.