• 专利标题:   Preparation of graphene quantum dot for use in e.g. optoelectronic device, involves hydrothermally reacting phloroglucinol solution, cooling, and centrifuging to obtain supernatant as aqueous solution of graphene quantum dots.
  • 专利号:   CN111072013-A
  • 发明人:   CHEN W, LV G, SHEN J, LI D, LI Y, LIU X, DAI Z
  • 专利权人:   UNIV CHINA THREE GORGES
  • 国际专利分类:   C01B032/184, C09K011/65
  • 专利详细信息:   CN111072013-A 28 Apr 2020 C01B-032/184 202043 Pages: 9 Chinese
  • 申请详细信息:   CN111072013-A CN11341481 24 Dec 2019
  • 优先权号:   CN11341481

▎ 摘  要

NOVELTY - Preparation of graphene quantum dot, involves adding phloroglucinol solution to a hydrothermal reactor, placing in a blast dryer, reacting at 160-220 degrees C for 2-15 hours, preferably at 180 degrees C for 8 hours, cooling naturally to obtain a brownish yellow solution, adding the solution to a centrifugal tube, and centrifuging at 3000-15000 rpm to obtain a brownish yellow clear and transparent supernatant as aqueous solution of graphene quantum dots. USE - Preparation of graphene quantum dots for use in optoelectronic device and biomedicine. ADVANTAGE - The method does not use a strong acid or strong alkali oxidant or any other chemical reagents, is simple, efficient, safe and environmentally-friendly, and can be carried out industrially on a large scale. The obtained graphene quantum dots have stable fluorescence, and excellent water solubility and biocompatibility.