• 专利标题:   Preparing sulfonated grapheme useful in energy storage comprises preparing saccharified graphene powder, ultrasonically dispersing into dichloromethane solution, adding chlorosulfonic acid, stirring reaction, washing and freeze-drying.
  • 专利号:   CN110668431-A
  • 发明人:   WANG L, ZHU K, TIAN H, TAN Y, ZHANG R, YU Z, LI W, HE Y, LAI Y
  • 专利权人:   UNIV YANSHAN
  • 国际专利分类:   C01B032/184, C01B032/194
  • 专利详细信息:   CN110668431-A 10 Jan 2020 C01B-032/184 202009 Pages: 12 Chinese
  • 申请详细信息:   CN110668431-A CN11137240 19 Nov 2019
  • 优先权号:   CN11137240

▎ 摘  要

NOVELTY - Preparing sulfonated grapheme comprises (i) mixing graphene oxide aqueous solution and glucosamine, and adjusting the pH value to be greater than 8, and reacting at 40-100 degrees C, carrying out ultrasonication for 4-12 hours, suction filtration, washing, and freeze drying to obtain saccharified graphene powder, (ii) ultrasonically dispersing the saccharified graphene obtained above into a dichloromethane solution to obtain saccharified graphene dispersion, adding chlorosulfonic acid to the dispersion, stirring reaction, and washing and freeze-drying. USE - The sulfonated graphene is useful in energy storage (claimed). ADVANTAGE - The method: improves the abundance of the hydrophilic structure in the sulfonated graphene, improve the dispersion of sulfonated graphene in various solvent systems; and sulfonated graphene has high capacity and excellent stability. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for sulfonated graphene prepared by the preparation method.