• 专利标题:   Preparing nitrogen-doped graphene material involves using di-amino azofurazan, dispersing graphene in water and adding solution of diamino azofuran in ethanol and heating, cooling and drying to diamino azofurazan eutectic.
  • 专利号:   CN108101037-A, WO2019119459-A1
  • 发明人:   ZHUO H, CHEN S, ZHU J
  • 专利权人:   UNIV SHENZHEN, UNIV SHENZHEN
  • 国际专利分类:   C01B032/194
  • 专利详细信息:   CN108101037-A 01 Jun 2018 C01B-032/194 201846 Pages: 8 Chinese
  • 申请详细信息:   CN108101037-A CN11410939 23 Dec 2017
  • 优先权号:   CN11410939, WOCN118139

▎ 摘  要

NOVELTY - Preparing nitrogen-doped graphene material involves using di-amino azofurazan, dispersing graphene in water and adding solution of diamino azofuran in ethanol and heating at 50-70 degrees C for 30-60 minutes, cooling at 20-40 degrees C, and drying to obtain graphene-coated diamino azofurazan eutectic, where mass ratio of diamino group in the solution of graphene and diamino azofurazan is 1:1-10. The diamino azofurazide eutectic is ground into a powder and heated at 500-800 degrees C for 3-5 hours to obtain nitrogen-doped graphene material. USE - Method for preparing nitrogen-doped graphene material. ADVANTAGE - The method enables to prepare nitrogen-doped graphene material which has high nitrogen doping content of graphene material which are uniformly coated on surface of diamino-4,4'-azoxyfurazan crystal which is free of any adhesive and other auxiliary agent, and keeps azo furoxan crystal surface properties.