• 专利标题:   Graphene-modified tin dioxide electrocatalyst comprises graphene and tin dioxide at specified mass ratio.
  • 专利号:   CN102205239-A, CN102205239-B
  • 发明人:   CHEN J, FEI X, LI S, WANG W, WU Y, YANG S, ZHAO Y, ZHOU M, ZHU T
  • 专利权人:   UNIV CHANGAN
  • 国际专利分类:   A62D101/28, A62D003/115, B01J023/14
  • 专利详细信息:   CN102205239-A 05 Oct 2011 B01J-023/14 201214 Pages: 6 Chinese
  • 申请详细信息:   CN102205239-A CN10084032 03 Apr 2011
  • 优先权号:   CN10084032

▎ 摘  要

NOVELTY - Graphene-modified tin dioxide electrocatalyst comprises graphene and tin dioxide at 0.1-2.5:1000 mass ratio. USE - Graphene-modified tin dioxide electrocatalyst. ADVANTAGE - The preparation of electrocatalyst is simple with low cost; and protects graphene to a maximum degree. The electrocatalyst has greatly improved catalytic efficiency and stable property; and can be reused. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparation of graphene-modified tin dioxide electrocatalyst comprising: (A) preparing graphene-stannic chloride sol by adding 0.5-15 mg graphene into 20-100 ml of 5-40 mass% stannic chloride solution; uniformly shaking the solution and ultrasonically dispersing for 20-30 minutes; stirring the solution with a constant temperature magnetic heating stirrer; and dropping 0.3-5 mol/L ammonia water at 20-30 drops/minute during the stirring operation until colorless and transparent graphene-stannic chloride sol is obtained; and (B) preparing the catalyst by standing and aging the graphene-stannic chloride sol for 10-18 hours; drying at 30-60 degrees C; placing into a muffle furnace; baking at 400-600 degrees C for 2-4 hours; after the furnace is cooled at room temperature, grinding the materials in a mortar; and screening the materials through a 100-mesh screen to obtain graphene-modified tin dioxide electrocatalyst.