• 专利标题:   Preparation of graphene comprises mixing graphite oxide and tetrahydrofuran, ultrasonically treating, reducing oxidized graphite alkene in graphene oxide suspension, adding lithium aluminum hydride, and dripping phosphorus tribromide.
  • 专利号:   CN102408110-A, CN102408110-B
  • 发明人:   LI Z, LIU D, LIU H, LUO Y, MA L, TANG Z, YAN J
  • 专利权人:   DONGGUAN MAIKE SCI TECHNOLOGY CO LTD, MCNAIR NEW POWER CO LTD, DONGGUAN MCNAIR INST LITHIUM ION BATTERY IND ENERGY SAVING, LITHIUM ION BATTERY IND ENERGYSAVING
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN102408110-A 11 Apr 2012 C01B-031/04 201278 Pages: 7 Chinese
  • 申请详细信息:   CN102408110-A CN10409936 09 Dec 2011
  • 优先权号:   CN10409936

▎ 摘  要

NOVELTY - Preparation of graphene comprises mixing graphite oxide and tetrahydrofuran to prepare suspension, ultrasonically treating for 25-35 minutes to obtain brown oxide graphene suspension, reducing oxidized graphite alkene in graphene oxide suspension, adding lithium aluminum hydride, stirring at room temperature for 24 hours, filtering and drying to obtain reduction of graphite oxide; and reducing graphite oxide with dichloromethane, for 25-35 minutes, dripping phosphorus tribromide into suspension after ultrasonic, stirring and reacting for 24 hours, filtering, washing and drying. USE - Method of preparation of graphene (claimed). ADVANTAGE - The method is simple and easy.