• 专利标题:   Preparation of nanohydroxyapatite/graphene-based composite material used e.g. for bone tissue repair involves adding graphene oxide powder to calcium salt, stirring adjusting pH, dripping phosphate solution, reacting, aging and filtering.
  • 专利号:   CN107161969-A, CN107161969-B
  • 发明人:   CHEN Q, YANG Z, YAN T, LIU J
  • 专利权人:   UNIV KUNMING SCI TECHNOLOGY, UNIV KUNMING SCI TECHNOLOGY
  • 国际专利分类:   A61L027/12, A61L027/42, A61L027/50, C01B025/32, C01B032/198
  • 专利详细信息:   CN107161969-A 15 Sep 2017 C01B-025/32 201771 Pages: 11 Chinese
  • 申请详细信息:   CN107161969-A CN10425341 08 Jun 2017
  • 优先权号:   CN10425341

▎ 摘  要

NOVELTY - Preparation of nanohydroxyapatite/graphene-based composite material comprises adding graphene oxide powder to calcium salt, and stirring in water bath at 30-50 degrees C; adjusting pH using ammonia solution to 9.5-10.5, dripping phosphate solution, and reacting at 30-50 degrees C; stirring for 16-24 hours at 35-40 degrees C, and aging at room temperature for 12-24 hours; and standing, repeatedly washing with deionized water until neutral, filtering, and freeze-drying. USE - Method for preparing nanohydroxyapatite/graphene-based composite material (claimed) used for bone tissue repair and dental restoration. ADVANTAGE - The method is simple and controllable with low cost, short processing period and low energy consumption. The material has good biocompatibility and oxidization.