• 专利标题:   Preparation of precursor used for preparing nickel iron phosphate anode material, involves mixing iron, nickel and phosphorus source solutions, adjusting pH of mixed solution using ammonia water, and spraying and drying mixed solution.
  • 专利号:   CN114105117-A
  • 发明人:   ZHANG W, CHEN D, LIU H
  • 专利权人:   HEFEI GUOXUAN HIGH TECH POWER SOURCE CO
  • 国际专利分类:   B82Y030/00, B82Y040/00, C01B025/45, H01M010/0525, H01M004/58, H01M004/62
  • 专利详细信息:   CN114105117-A 01 Mar 2022 C01B-025/45 202255 Chinese
  • 申请详细信息:   CN114105117-A CN11220730 20 Oct 2021
  • 优先权号:   CN11220730

▎ 摘  要

NOVELTY - Preparing precursor comprises (i) fully mixing iron source solution, nickel source solution and phosphorus source solution to obtain a first mixed solution, (ii) adjusting the pH of the first mixed liquid to 2-3 by using ammonia water, (iii) fully stirring at 10-80degrees Celsius to obtain second mixed liquid, (iv) spraying and drying the second mixed fluid to obtain precursor, (v) preparing nickel iron phosphate compound (I), and (vi) preparing a second mixed solution by fully mixing the nickel-iron phosphate solution and the phosphorus phosphate solution. USE - Preparation of precursor used for preparing nickel iron phosphate anode material. ADVANTAGE - The precursor obtained by the preparation method is more environment-friendly, the risk of safety in the production is lower, it can effectively increase the connection performance of the precursor particles, it is easy to realize industrial batch preparation of precursor, it provides support for the preparation of subsequent nickel iron phosphate. DETAILED DESCRIPTION - Preparing precursor comprises (i) fully mixing iron source solution, nickel source solution and phosphorus source solution to obtain a first mixed solution, (ii) adjusting the pH of the first mixed liquid to 2-3 by using ammonia water, (iii) fully stirring at 10-80degrees Celsius to obtain second mixed liquid, (iv) spraying and drying the second mixed fluid to obtain precursor, (v) preparing nickel iron phosphate compound of formula NixFe1-xPO4 (I), and (vi) preparing a second mixed solution by fully mixing the nickel-iron phosphate solution and the phosphorus phosphate solution. x=0.2-0.5.5. An INDEPENDENT CLAIM is included for a preparation method of lithium nickel iron phosphate anode material including fully mixing lithium nickel phosphate powder, fast ion conductor, and graphene powder.