• 专利标题:   Preparation of graphene-based antimony sulfide material used for forming negative electrode, involves mixing antimony source solution and ethylene glycol, adding sodium borohydride and polyvinylpyrrolidone, and hydrothermally reacting.
  • 专利号:   CN111129489-A
  • 发明人:   HAN S, MA J, HU X, HUANG Y, KONG Y, LI Y, CHEN Y, WANG H, JIANG P
  • 专利权人:   SHANGHAI INST TECHNOLOGY
  • 国际专利分类:   H01M010/0525, H01M004/58, H01M004/62
  • 专利详细信息:   CN111129489-A 08 May 2020 H01M-004/58 202044 Pages: 9 Chinese
  • 申请详细信息:   CN111129489-A CN11207002 29 Nov 2019
  • 优先权号:   CN11207002

▎ 摘  要

NOVELTY - Preparation of graphene-based antimony sulfide anode material involves (i) adding the antimony source to the deionized water, stirring it evenly, adding ethylene glycol and stirring to obtain the solution (A), (ii) adding sodium borohydride to the solution (A) obtained in step (i), stirring well and adding polyvinylpyrrolidone and fully dissolving to obtain a solution (B), (iii) adding solution (B) in step (ii) to the lining of the hydrothermal kettle containing sulfur powder to perform hydrothermal reaction, after completing the reaction, separating solid and liquid, washing and drying to obtain antimony trisulfide, and (iv) hydrothermally combining antimony trisulfide and graphite oxide and freeze-drying. USE - Preparation of graphene-based antimony sulfide material used for forming negative electrode for lithium-ion battery (claimed). ADVANTAGE - The method enables simple and economical preparation of graphene-based antimony sulfide material having excellent electrochemical performance, and which is performed in mild condition. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for two-dimensional carbide crystal-based antimony sulfide anode material.