• 专利标题:   Preparation of perovskite composite phosphor involves adding cesium-lead halide and complex e.g. boron nitride, graphene, graphene oxide, silica, diatomite and metal-organic framework, to ball mil, adding surfactant, and milling.
  • 专利号:   CN106675559-A
  • 发明人:   SONG J, DONG Y, XUE J, HAN B, LI J, XU L, ZENG H
  • 专利权人:   UNIV NANJING SCI TECHNOLOGY
  • 国际专利分类:   C09K011/02, C09K011/66
  • 专利详细信息:   CN106675559-A 17 May 2017 C09K-011/66 201749 Pages: 9 Chinese
  • 申请详细信息:   CN106675559-A CN11223726 27 Dec 2016
  • 优先权号:   CN11223726

▎ 摘  要

NOVELTY - Preparation of perovskite composite phosphor involves weighing cesium-lead halide (I) as raw material, adding the cesium-lead halide and a complex chosen from boron nitride, graphene, graphene oxide, silica, polyvinylpyrrolidinone, diatomite and metal-organic framework, to a ball mil, adding a surfactant chosen from oleylamine, oleic acid, n-octylamine and bis(dodecyldimethylammonium bromide), sealing the ball mill, and milling at 300-500 rpm for 2-24 hours. USE - Preparation of perovskite composite phosphor (claimed). ADVANTAGE - The method enables efficient preparation of perovskite composite phosphor with high yield and stability, by simple and economical process without requiring subsequent purification. DETAILED DESCRIPTION - Preparation of perovskite composite phosphor involves weighing cesium-lead halide of formula: CsPbXY'2 (I) as raw material, adding the cesium-lead halide and a complex chosen from boron nitride, graphene, graphene oxide, silica, polyvinylpyrrolidinone, diatomite and metal-organic framework, to a ball mil, adding a surfactant chosen from oleylamine, oleic acid, n-octylamine and bis(dodecyldimethylammonium bromide), sealing the ball mill, and milling at 300-500 rpm for 2-24 hours. X,Y'=Br, Cl or I.