• 专利标题:   Preparation of graphene by soaking graphite in acid and base solution, washing with deionized water, filtering, drying, heating, transferring to cylinder containing liquid nitrogen or hydrogen, evaporating, heating, and cooling.
  • 专利号:   CN103449409-A, CN103449409-B
  • 发明人:   WANG Y, YUAN X, ZHOU M
  • 专利权人:   OCEAN S KING LIGHTING SCI TECHNOLOGY, SHENZHEN OCEAN S KING LIGHTING SCI TECH, OCEANS KING LIGHTING SCI TECHNOLOGY CO, SHENZHEN OCEANS KING LIGHTING SCI TECH
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103449409-A 18 Dec 2013 C01B-031/04 201414 Pages: 7 Chinese
  • 申请详细信息:   CN103449409-A CN10173689 30 May 2012
  • 优先权号:   CN10173689

▎ 摘  要

NOVELTY - Preparation of graphene comprises soaking graphite in acid and alkali solution, washing with deionized water to neutralized, filtering, and drying; placing in muffle furnace, heating to 800-1000 degrees C under protective gas atmosphere, and incubating for 3-5 minutes; and transferring graphite with liquid inert gas to cylinder containing liquid nitrogen or liquid hydrogen, evaporating gas, placing graphite in muffle furnace, heating to 800-1000 degrees C, taking out, cooling, and collecting solid product. USE - Method for preparation of graphene (claimed). ADVANTAGE - The method is environment-friendly, simple, and suitable for large-scale industrial production, and has wide source of raw material and low cost.