• 专利标题:   Preparation of magnetic graphene oxide adsorbent for treating wastewater, involves preparing magnetic graphene oxide solid using graphene oxide, ferrous ion, ferric ion, and aqueous ammonia, reacting with aminothiourea, and centrifuging.
  • 专利号:   CN111229167-A
  • 发明人:   GE H, ZHA S
  • 专利权人:   UNIV SOUTH CHINA TECHNOLOGY
  • 国际专利分类:   B01J020/22, B01J020/28, B01J020/30, C02F001/28, C02F101/20
  • 专利详细信息:   CN111229167-A 05 Jun 2020 B01J-020/22 202053 Pages: 8 Chinese
  • 申请详细信息:   CN111229167-A CN10064608 20 Jan 2020
  • 优先权号:   CN10064608

▎ 摘  要

NOVELTY - Preparation of aminothiourea-modified magnetic graphene oxide adsorbent involves mixing (S1) graphene oxide, ferrous ion, ferric ion, and water to obtain a mixed solution, adding (S2) aqueous ammonia to the mixed solution, reacting at 70-90 degrees C for 50-70 minutes, centrifuging, washing, drying to obtain a magnetic ferroferric oxide and graphene oxide composite which is a magnetic graphene oxide solid, reacting (S3) the magnetic graphene oxide solid with aminothiourea using water as a reaction medium at 45-55 degrees C for 12-16 hours, centrifuging, washing, and drying. USE - Preparation of aminothiourea-modified magnetic graphene oxide adsorbent used for treating wastewater containing heavy metal ions e.g. divalent mercury ion (all claimed). ADVANTAGE - The method produces aminothiourea-modified magnetic graphene oxide adsorbent having excellent adsorption and desorption performance, regeneration characteristics, and mercury-ion selectivity, and large specific surface area.