• 专利标题:   Method for preparing anode material of lithium ion battery, involves dispersing graphene oxide in deionized water, adding hydrochloric acid and mixing, and dissolving stannous chloride in obtained solution, followed by reacting and washing.
  • 专利号:   CN104659367-A
  • 发明人:   DENG Y, LI Z, SONG X, ZHANG Z, ZHANG X, ZHENG X, ZHOU X, QU D, HUANG X
  • 专利权人:   DONGGUAN MAIKE SCI TECHNOLOGY CO LTD, MCNAIR NEW POWER CO LTD
  • 国际专利分类:   B82Y030/00, H01M004/48, H01M004/587
  • 专利详细信息:   CN104659367-A 27 May 2015 H01M-004/587 201558 Pages: 14 Chinese
  • 申请详细信息:   CN104659367-A CN10116470 17 Mar 2015
  • 优先权号:   CN10116470

▎ 摘  要

NOVELTY - An anode material preparing method involves dispersing graphene oxide in deionized water, adding hydrochloric acid and mixing to obtain a solution-A, and dissolving stannous chloride in the solution-A by mixing to obtain solution-B, which is reacted and washed to obtain graphene-stannic oxide composite material, which is dispersed in deionized water to form solution-C, followed by dissolving water-soluble polymeric substance in the solution-C to obtain solution-D. The solution-D is transferred into a reaction vessel to obtain reacted product, which is cooled, washed, dried and sintered. USE - Method for preparing an anode material of lithium ion battery. ADVANTAGE - The method enables preparing the anode material with increased lithium storage capacity, better effect of permeating electrolyte, increased electric conductivity and increased performance. DETAILED DESCRIPTION - An anode material preparing method involves dispersing graphene oxide in deionized water, adding hydrochloric acid and uniformly mixing to obtain a solution-A, and dissolving stannous chloride in the solution-A by mixing to obtain solution-B. The solution-B is reacted at 40-80 degrees C for 4-12 hours and washed to obtain graphene-stannic oxide composite material. The obtained composite material is dispersed in deionized water to form solution-C, followed by dissolving water-soluble polymeric substance in the solution-C by mixing to obtain solution-D. The solution-D is transferred into a reaction vessel. The reaction vessel is placed in an environment at 160-200 degrees C for 2-12 hours to obtain reacted product. The reacted product is cooled, washed, dried in 10-1000 ppm protective atmosphere containing oxygen and inert gas, and sintered at 700-800 degrees C to obtain finished product.