• 专利标题:   Synthesis of graphene by adding iron ion-loaded montmorillonite catalyst and benzene into crucible, putting in high pressure reaction kettle, controlling temperature, and washing product with hydrofluoric acid and nitric acid mixed solution.
  • 专利号:   CN103601176-A, CN103601176-B
  • 发明人:   GU C, GUO Y
  • 专利权人:   UNIV NANJING
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103601176-A 26 Feb 2014 C01B-031/04 201429 Pages: 19 Chinese
  • 申请详细信息:   CN103601176-A CN10573152 15 Nov 2013
  • 优先权号:   CN10573152

▎ 摘  要

NOVELTY - Synthesis of graphene comprises adding iron ion (Fe3+)-loaded montmorillonite catalyst and benzene into crucible, putting in high pressure reaction kettle, controlling the temperature at 150-350 degrees C for 4-5 hours, washing the product with hydrofluoric acid and nitric acid mixed solution under ultrasonic condition to remove montmorillonite framework, and freeze drying to obtain graphene black powder. USE - Synthesis of graphene (claimed). ADVANTAGE - The method does not need carrier gas during the reaction and has low reaction temperature and low reaction cost.