▎ 摘　　要

NOVELTY - Preparing anode/cathode material involves adding sodium molybdate and thiourea into the solvent, stirring uniformly to form a mixed solution, in the mixed solution, adding graphene oxide (GO) solution, and ultrasonically dispersing to form solution (A), and dispersing selenium powder in hydrazine hydrate solution to form solution (B). The solution (A) and solution (B) are mixed, performed a hydrothermal reaction, and freeze-dried to obtain a composite electrode material aerogel. The sulfur is carried in the composite electrode material aerogel to obtain anode material or the composite electrode material aerogel is loaded with lithium to obtain cathode material. USE - Method for preparing anode/cathode material for a lithium-sulfur battery. ADVANTAGE - The method prepared anode/cathode material with high performance.