• 专利标题:   Preparing polyborosiloxane modified polyurethane aqueous coating, comprises e.g. dissolving borate in water, adding chlorosilane dropwise, stirring, reacting, drying, adding polydimethylsiloxane, and controlling molar ratio of boron and silicon.
  • 专利号:   CN114958171-A
  • 发明人:   XIA Y, LIU X
  • 专利权人:   LIU X
  • 国际专利分类:   C08G018/32, C08G018/34, C08G018/61, C08G018/65, C09D175/04, C09D007/62
  • 专利详细信息:   CN114958171-A 30 Aug 2022 C09D-175/04 202291 Chinese
  • 申请详细信息:   CN114958171-A CN10642735 08 Jun 2022
  • 优先权号:   CN10642735

▎ 摘  要

NOVELTY - Preparing polyborosiloxane modified polyurethane aqueous coating comprises dissolving borate in water, adding chlorosilane dropwise, stirring, reacting, drying, adding polydimethylsiloxane, adjusting the amount of raw materials added, controlling molar ratio of boron and silicon in borosiloxane prepolymer to obtain variety of borosiloxane prepolymers with different molar ratios, where the borosiloxane prepolymers with different molar ratio comprises (a) borosiloxane prepolymer with molar ratio of boron and silicon is 1:50, (b) borosiloxane prepolymer with molar ratio of boron and silicon is 1:30, and (c) borosiloxane prepolymer with molar ratio of boron and silicon is 1:10, taking isocyanate, borosiloxane prepolymer (a), (b) and (c), and dibutyltin dilaurate, performing reaction at 40-50℃, adding polyol, heating at 80-85℃, adding diethylene glycol and dimethylol propionic acid, continuing reaction, adding triethylamine for neutralization, discharging and emulsifying. USE - The method is useful for preparing polyborosiloxane modified polyurethane aqueous coating. ADVANTAGE - The method enables to prepare polyborosiloxane modified polyurethane aqueous coating, which has excellent water resistance and water resistance.