• 专利标题:   Preparation of graphene-supported titania involves ultrasonically dispersing graphene oxide to obtain dispersion, transferring dispersion to constant temperature water bath, magnetically stirring and dripping titanium chloride solution.
  • 专利号:   CN106423129-A
  • 发明人:   LIN C, XUE D, ZHOU L, CHANG M, YANG X
  • 专利权人:   UNIV XIAN SHIYOU
  • 国际专利分类:   B01J021/18, B01J037/10, B82Y030/00
  • 专利详细信息:   CN106423129-A 22 Feb 2017 B01J-021/18 201726 Pages: 10 Chinese
  • 申请详细信息:   CN106423129-A CN10709773 23 Aug 2016
  • 优先权号:   CN10709773

▎ 摘  要

NOVELTY - The preparation method of graphene-supported titania involves (1) ultrasonically dispersing 100 ml of 200-300 mg/l graphene oxide to obtain dispersion, (2) transferring the dispersion of step (1) to constant temperature water bath, magnetically stirring, dripping titanium chloride solution, adding nonylphenol ethoxylate surfactant, reacting for 120 minutes, cooling the mixture, (3) pouring mixture obtained in step (2) into hydrothermal reactor, heating, cooling, centrifuging, washing with distilled water and anhydrous ethanol and drying to obtain black solid particles. USE - Preparation of graphene-supported titania (claimed). ADVANTAGE - The method enables preparation of graphene-supported titania by simple and safe process. DETAILED DESCRIPTION - The preparation method of graphene-supported titania involves (1) ultrasonically dispersing 100 ml of 200-300 mg/l graphene oxide for 60 minutes to obtain dispersion, (2) transferring the dispersion of step (1) to 45-80 degrees C constant temperature water bath, magnetically stirring, dripping 25-35% of 1-2 ml titanium chloride solution, adding 0.5 ml nonylphenol ethoxylate surfactant, reacting for 120 minutes, cooling the mixture, (3) pouring the mixture obtained in step (2) into 150 ml hydrothermal reactor, heating at 150-180 degrees C for 8-10 hours, naturally cooling, centrifuging, washing with distilled water and anhydrous ethanol 2-3 times and drying at 80-90 degrees C to obtain black solid particles.