• 专利标题:   Preparing high-quality water-soluble graphene involves adding deionized water and graphene to a round bottom flask, persulfate after magnetic stirring at room temperature, and replacing with ultrapure nitrogen to remove oxygen.
  • 专利号:   CN111874898-A
  • 发明人:   HAN L, ZHONG Y
  • 专利权人:   QINGDAO OLEFINIC CARBON RUIER NEW MATERI
  • 国际专利分类:   C01B032/194
  • 专利详细信息:   CN111874898-A 03 Nov 2020 C01B-032/194 202002 Pages: 8 Chinese
  • 申请详细信息:   CN111874898-A CN10785866 03 Aug 2020
  • 优先权号:   CN10785866

▎ 摘  要

NOVELTY - Preparing high-quality water-soluble graphene involves adding deionized water and graphene to a round bottom flask, persulfate after magnetic stirring for a period of time at room temperature, and replacing with ultrapure nitrogen to remove oxygen (O2) and carbon dioxide (CO2) dissolved in deionized water. The metal ion aqueous solution is continuously dropped into the reaction flask through a constant pressure funnel, and the persulfate anion (S2O82-) is activated to produce sulfate radicals and continuously oxidize the edges of the graphene. The edge graphene oxide obtained is sequentially subjected to ultrasonic treatment and centrifugal washing to obtain stable dispersion of graphene dispersion. USE - Method for preparing high-quality water-soluble graphene. ADVANTAGE - The method enables to prepare high-quality water-soluble graphene in a simple manner and graphene is in powder form, has excellent conductivity and mechanical performance, and thickness of less than equal to 3mm.