• 专利标题:   High-efficient transposition washing method for preparing thin layer graphene, involves thermally expanding prepared impurity-containing graphite oxide powder to obtain impurity-containing graphene, washing and spray-drying or vacuum-drying.
  • 专利号:   CN115448298-A
  • 发明人:   GUO X, LIU J, LI D, DONG F, YU N, ZHANG Y, ZHAO W, SUN B, ZONG J
  • 专利权人:   TIANJIN VOCATIONAL INST
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN115448298-A 09 Dec 2022 C01B-032/184 202311 Chinese
  • 申请详细信息:   CN115448298-A CN11173541 26 Sep 2022
  • 优先权号:   CN11173541

▎ 摘  要

NOVELTY - A high-efficiency transposition washing method involves preparing graphite oxide, optionally washing the graphite oxide by low-speed centrifuge, crushing to obtain impurity-containing graphite oxide powder, thermally expanding the graphite oxide powder to obtain an impurity-containing graphene, repeatedly washing the graphene by rapid solid/liquid separation, and spray-drying or vacuum-drying the wet graphene at room temperature to obtain pure thin-layer graphene powder. USE - High-efficiency transposition washing method for preparing thin layer graphene used as carbon material in lithium-ion battery, electrochemical capacitor and fuel cell. ADVANTAGE - The method is simple, fast, time-saving and easy, ensures low energy consumption and mass production of thin-layer graphene, improves the whole preparation efficiency of the thin layer graphene, avoids sol-gel of graphite oxide, and ensures easy washing and purifying processes.