• 专利标题:   Manufacture of ionic liquid-modified graphene oxide-natural rubber vulcanized rubber involves preparing ionic liquid-modified graphene oxide, mixed with natural rubber, zinc oxide, antioxidant, curing agent and stearic acid and cured.
  • 专利号:   CN103102514-A, CN103102514-B
  • 发明人:   JIA H, XU J, TANG Y, XIONG X, LI F, WU T, WANG J, LIU P, ZHANG J, ZHANG X, HE Z, XU Z
  • 专利权人:   UNIV NANJING SCI TECHNOLOGY
  • 国际专利分类:   C08K013/06, C08K003/04, C08K003/06, C08K003/22, C08K005/09, C08K009/02, C08K009/04, C08L007/00
  • 专利详细信息:   CN103102514-A 15 May 2013 C08L-007/00 201413 Pages: 9 Chinese
  • 申请详细信息:   CN103102514-A CN10035966 30 Jan 2013
  • 优先权号:   CN10035966

▎ 摘  要

NOVELTY - Graphite oxide is prepared. The obtained graphite oxide is crushed to powder using agate mortar, ionic liquid-acetone solution is added and dried in oven, to obtain ionic liquid-modified graphene oxide. Natural rubber is masticated using double-roller. Obtained natural rubber, zinc oxide, stearic acid, vulcanization accelerators, antioxidants, curing agent, plasticizer, ionic liquid-modified graphene oxide and carbon black are mixed in open mixing machine or internal mixer and cured, to obtain ionic liquid-modified graphene oxide-natural rubber vulcanized rubber. USE - Manufacture of ionic liquid-modified graphene oxide-natural rubber vulcanized rubber. ADVANTAGE - The method provides ionic liquid-modified graphene oxide-natural rubber vulcanized rubber having improved heat conduction coefficient and mechanical properties, by simple process. DETAILED DESCRIPTION - Graphite and sodium nitrate are added to concentrated sulfuric acid, stirred, potassium permanganate is added, deionized water and hydrogen peroxide solution are added, filtered, washed with deionized water and hydrochloric acid, respectively, and dried, to obtain graphite oxide. The obtained graphite oxide is crushed to powder using agate mortar, ionic liquid-acetone solution is added and dried in oven, to obtain ionic liquid-modified graphene oxide. Natural rubber is masticated using double-roller. Obtained natural rubber, zinc oxide, stearic acid, vulcanization accelerators, antioxidants, curing agent, plasticizer, ionic liquid-modified graphene oxide and carbon black are mixed in open mixing machine or internal mixer and cured, to obtain ionic liquid-modified graphene oxide-natural rubber vulcanized rubber.