• 专利标题:   Preparing viscose fiber, by adding sodium hydroxide to aqueous dispersion of graphene oxide, adding nano-carbon black, and mixing to obtain mixed dispersion, and adding viscose spinning solution to mixed dispersion, forming and packing.
  • 专利号:   CN110424060-A
  • 发明人:   CHEN C, HAN Y, GAO C
  • 专利权人:   HANGZHOU GAOXI TECHNOLOGY CO LTD
  • 国际专利分类:   D01F002/08
  • 专利详细信息:   CN110424060-A 08 Nov 2019 D01F-002/08 201990 Pages: 9 Chinese
  • 申请详细信息:   CN110424060-A CN10837159 05 Sep 2019
  • 优先权号:   CN10837159

▎ 摘  要

NOVELTY - Method for preparing a nanocarbon black modified viscose fiber, involves (a) adding 0.01 part mass sodium hydroxide to 25 parts mass aqueous dispersion of graphene oxide having concentration of 2 mg/g, mixing and stirring to obtain mixed solution, (b) mixing low dibutyl phthalate value nano-carbon black and high dibutyl phthalate value nano-carbon black in a mass ratio of 3-5:1 to obtain mixed nano-carbon black, and adding 0.12-0.2 part mass mixed nano-carbon black to obtained mixed solution, and stirring at 100 degrees C for 1 hour to obtain mixed dispersion, where the dibutyl phthalate value of the high dibutyl phthalate value nano-carbon black is 360-400, and the dibutyl phthalate value of low dibutyl phthalate value nano-carbon black is 200-280, and (c) adding 100 parts mass viscose spinning solution having 9-12 wt.% nail fiber to the mixed dispersion, and uniformly mixing, forming, holding, washing, desulfurizing, oiling, spinning in a coagulation bath by spinneret, drying and packing. USE - The method is used for preparing nanocarbon black modified viscose fiber. ADVANTAGE - The method maintains excellent dispersion, anti-static function, anti-UV effect and anti-bacterial property, has stable function and does not decay with water washing.