• 专利标题:   Preparing graphene nano-cavitation microspheres by dissolving paraffin and emulsifier in aqueous phase solvent, dispersing graphene in tetrahydrofuran solution, mixing with degassed water, reacting, mixing paraffin microcapsules with graphene solution and using paraffin capsules as sacrificial layer.
  • 专利号:   CN115957705-A
  • 发明人:   ZHAO Z, LI Z, LIU Y, ZONG G
  • 专利权人:   SHANDONG RARE TECHNOLOGY DEV CO LTD
  • 国际专利分类:   B01J013/02, B01J020/20, B01J020/28, B01J020/30
  • 专利详细信息:   CN115957705-A 14 Apr 2023 B01J-013/02 202343 Chinese
  • 申请详细信息:   CN115957705-A CN11637322 16 Dec 2022
  • 优先权号:   CN11637322

▎ 摘  要

NOVELTY - Preparing graphene nano-cavitation microspheres comprises (1) dissolving the paraffin and emulsifier in the aqueous phase solvent, and stirring at a constant temperature and rotating speed for a certain period of time to form a stable oil-in-water emulsion, where the precipitate after centrifugation at room temperature is paraffin microcapsules, (2) dispersing graphene in tetrahydrofuran solution and mixing with degassed water, reacting for a certain period of time, and removing the tetrahydrofuran by solvent evaporation to obtain a stable graphene solution dispersed in water, and (3) mixing the paraffin microcapsules with the graphene solution, fully stirring and then filtering, wrapping the graphene nanosheets on the paraffin surface, and finally drying at 60°C, using the paraffin capsules as a sacrificial layer to be heated and melted to remove to obtain hollow graphene nanocavitation microspheres. USE - The method is useful for preparing graphene nano-cavitation microspheres. ADVANTAGE - The graphene nanocavitation microspheres has broad spectrum and high adsorption capacity for various metal ions and soluble organic substances with fast adsorption rate.