• 专利标题:   Preparing nitrogen-doped porous graphene used for super capacitor, involves adding nano nickel powder dispersed in trisaminomethane hydrochloric acid buffer solution with dopamine concentration, and then oscillating obtained mixture.
  • 专利号:   CN106006614-A
  • 发明人:   SONG H, ZHAO D, LI F, DAI T, ZHOU P
  • 专利权人:   FUJIAN XIANGFENGHUA NEW ENERGY MATERIAL
  • 国际专利分类:   C01B031/04, H01G011/32
  • 专利详细信息:   CN106006614-A 12 Oct 2016 C01B-031/04 201710 Pages: 6 Chinese
  • 申请详细信息:   CN106006614-A CN10351306 25 May 2016
  • 优先权号:   CN10351306

▎ 摘  要

NOVELTY - Nitrogen-doped porous graphene preparation involves adding 3-10g nano nickel powder dispersed in 300-1000ml trisaminomethane hydrochloric acid buffer solution with the 0.1-5mg/ml dopamine concentration. The obtained mixture is ultrasonically oscillated. The obtained mixture is mechanically stirred at room temperature for 5-10 hours. The obtained stirred mixture is heated at 50 degrees C for 1-4 hours. The obtained mixture is rolled with 50 cm diameter roller. Nitrogen doped porous graphene precursor is prepared by mixing polydopamine as the solid precursor, nickel as catalyst and template. USE - Method for preparing nitrogen-doped porous graphene used for super capacitor (claimed). ADVANTAGE - The method enables to prepare nitrogen-doped porous graphene in a simple and cost-effective manner. DETAILED DESCRIPTION - Nitrogen-doped porous graphene preparation involves adding 3-10g nano nickel powder dispersed in 300-1000ml trisaminomethane hydrochloric acid buffer solution with the 0.1-5mg/ml dopamine concentration. The obtained mixture is ultrasonically oscillated. The obtained mixture is mechanically stirred at room temperature for 5-10 hours. The obtained stirred mixture is heated at 50 degrees C for 1-4 hours. The obtained mixture is rolled with 50 cm diameter roller. Nitrogen doped porous graphene precursor is prepared by mixing polydopamine as the solid precursor, nickel as catalyst and template. The obtained mixture is sintered in a sintering furnace at 800-1000 degrees C in presence of inert gas. The obtained mixture is cooled at room temperature. to form graphene doped with nitrogen product coated by the nickel sheet body. The obtained nickel sheet body is etched with strong acid and acid. The obtained product is washed, and then dried.