• 专利标题:   Preparing three-dimensional nitrogen and parathion doped graphene involves adding hydrotalcite to sodium butyrate, stirring mixture, warming mixture in water bath to obtain acid-modified hydrotalcite suspension, mixing with acetone.
  • 专利号:   CN104828801-A, CN104828801-B
  • 发明人:   HUANG W, HUANG Y
  • 专利权人:   UNIV CHANGZHOU
  • 国际专利分类:   C01B031/00
  • 专利详细信息:   CN104828801-A 12 Aug 2015 C01B-031/00 201578 Pages: 5 Chinese
  • 申请详细信息:   CN104828801-A CN10228997 07 May 2015
  • 优先权号:   CN10228997

▎ 摘  要

NOVELTY - Preparing three-dimensional nitrogen and parathion doped graphene involves adding hydrotalcite to sodium butyrate and stirring for 5-6 hours at 60-70 degrees C. The mixture is warmed in water bath for 12-24 hours to obtain acid-modified hydrotalcite suspension. The acetone, methyl parathion and acid-modified hydrotalcite suspension are mixed and mixture is stirred for 6-8 hours at 60-70 degrees C in water bath. The precipitate is separated from the liquid and then washed 2-3 times with deionized water. The mixture is dried and ground over 20-40 meshes sieve to obtain modified hydrotalcite. USE - Method for preparing three-dimensional nitrogen and parathion doped graphene (claimed). ADVANTAGE - The method enables to prepare three-dimensional nitrogen and parathion doped graphene in simple manner under mild conditions. DETAILED DESCRIPTION - Preparing three-dimensional nitrogen and parathion doped graphene involves adding hydrotalcite to sodium butyrate and stirring for 5-6 hours at 60-70 degrees C. The mixture is warmed in water bath for 12-24 hours to obtain acid-modified hydrotalcite suspension. The acetone, methyl parathion and acid-modified hydrotalcite suspension are mixed and mixture is stirred for 6-8 hours at 60-70 degrees C in water bath. The precipitate is separated from the liquid and then washed 2-3 times with deionized water. The mixture is dried and ground over 20-40 meshes sieve to obtain modified hydrotalcite. The modified hydrotalcite is transferred to the vacuum tube furnace and calcined under vacuum to 400-600 degrees C for 2-4 hours. The calcined powder is cooled to room temperature and added with 20-40% hydrochloric acid solution per gram of powder. The mixture is stirred for 3-4 hours under nitrogen and precipitated. The mixture is dried under the vacuum conditions and heated to 2000-2500 degrees C for 3-6 hours to obtain three-dimensional nitrogen and parathion doped graphene.