• 专利标题:   Preparation of beta-aminocarbonyl comprises reacting aromatic aldehyde, aromatic amine and ketone in water solvent and graphene oxide catalyst.
  • 专利号:   CN104496831-A, CN104496831-B
  • 发明人:   GAO Z, HE L, SUN H, ZHANG Y
  • 专利权人:   UNIV SHAANXI NORMAL
  • 国际专利分类:   C07C221/00, C07C225/18
  • 专利详细信息:   CN104496831-A 08 Apr 2015 C07C-221/00 201547 Pages: 9 Chinese
  • 申请详细信息:   CN104496831-A CN10841113 30 Dec 2014
  • 优先权号:   CN10841113

▎ 摘  要

NOVELTY - Preparation of beta -aminocarbonyl (I) or (II) comprises reacting aromatic aldehyde, aromatic amine and ketone in water solvent in the presence of graphene oxide catalyst at 50 degrees C for 3-6 hours. USE - Method for preparation of beta -aminocarbonyl (claimed). ADVANTAGE - The method is simple, uses environment-friendly, nontoxic and inexpensive catalyst, achieves high yield, recycles catalyst, and has mild reaction condition and short reaction time. DETAILED DESCRIPTION - Preparation of beta -aminocarbonyl of formula (I) or (II) comprises reacting aromatic aldehyde, aromatic amine and ketone in water solvent in the presence of graphene oxide catalyst at 50 degrees C for 3-6 hours. R1, R2=H, Cl, Br, methyl and/or methoxy; and m, n=0-2.