• 专利标题:   Preparing small sheet diameter graphene useful in polyethylene terephthalate composite material, comprises mixing graphite, water, glass microsphere, pyrene methanol and methanol for sand grinding, and settling graphene and glass microsphere mixed suspension, spraying and drying graphene solution.
  • 专利号:   CN116102005-A
  • 发明人:   LI Z, MEI Y, MA Y
  • 专利权人:   NINGBO TOPCENTRAL NEW MATERIAL CO LTD
  • 国际专利分类:   C01B032/19, C08K003/04, C08K009/02, C08K009/04, C08L067/02
  • 专利详细信息:   CN116102005-A 12 May 2023 C01B-032/19 202351 Chinese
  • 申请详细信息:   CN116102005-A CN11586140 09 Dec 2022
  • 优先权号:   CN11586140

▎ 摘  要

NOVELTY - Preparing small sheet diameter graphene comprises mixing the graphite, water, glass microsphere, 1-pyrene methanol and methanol for sand grinding to obtain graphene/glass microsphere mixed suspension, where the glass bead includes a first glass bead, a second glass bead, a third glass bead and a fourth glass bead, the particle size of the first glass microspheres, the second glass microspheres, the third glass microspheres and the fourth glass microspheres is 400-600 μm, 150-300 μm, 50-100 μm and 1-40 μm, the mass ratio of the first glass microsphere, the second glass microsphere, the third glass microsphere and the fourth glass microsphere is 1-2:2-3:4-16:8-20, allowing to stand and settling graphene/glass microsphere mixed suspension to obtain the upper graphene of the suspension, spraying and drying graphene suspending solution. USE - The method is useful in polyethylene terephthalate composite material (claimed). ADVANTAGE - The method improves the mechanical property and conductivity of polyethylene terephthalate material. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are also included for: the small sheet diameter graphene prepared by above method; a polyethylene terephthalate composite material comprising 5-45 pts. wt. graphene, 50-90 pts. wt. polyethylene terephthalate, 0.003-0.01 pts. wt. chain extension and 0.003-0.01 pts. wt. antioxidant , where graphene is the small sheet diameter graphene; and a method for preparing polyethylene terephthalate composite material comprising mixing graphene, polyethylene terephthalate, chain extender and antioxidant for double-screw extruding .