• 专利标题:   Industrial electrolytic stripping preparation of graphene composite material by taking two high-purity graphite rods as electrolytic cathode and anode, taking polymer or biomolecule as electrolyte, and conducting electrolytic stripping.
  • 专利号:   CN102206388-A, CN102206388-B
  • 发明人:   QU P, LI C, XU M, ZHU X
  • 专利权人:   UNIV SHANGQIU
  • 国际专利分类:   C08K003/04, C08L025/18, C08L039/06, C08L005/08, C08L005/16, C08L089/00
  • 专利详细信息:   CN102206388-A 05 Oct 2011 C08L-025/18 201205 Chinese
  • 申请详细信息:   CN102206388-A CN10121687 12 May 2011
  • 优先权号:   CN10121687

▎ 摘  要

NOVELTY - Industrial electrolytic stripping preparation of graphene composite material comprises taking two 99.999% high-purity graphite rods as electrolytic cathode and anode; taking polymer or biomolecule as electrolyte; and under the condition of electrolytic additives, fast mixing, and constant direct voltage of 4-16V, electrolytic stripping high-purity graphite rod to obtain high-quality graphene composite material. The polymer or biomolecule is 1-ethoxy-3-methylimidazole sodium polystyrene benzene sulfonate, polyvinyl pyrrolidone, beta -cyclodextrin, chitosan, DNA, RNA, polypeptide, or protein. USE - Industrial electrolytic stripping preparation of graphene composite material (claimed) used for modifying electrode as biological sensor. ADVANTAGE - The method provides high-quality graphene composite material; needs only one direct-current potentiostat; has small investment, low cost, easily controlled reaction process, and no pollution; and is simple. DETAILED DESCRIPTION - Industrial electrolytic stripping preparation of graphene composite material comprises taking two 99.999% high-purity graphite rods as electrolytic cathode and anode; taking polymer or biomolecule as electrolyte; and under the condition of electrolytic additives, fast mixing, and constant direct voltage of 4-16V, electrolytic stripping high-purity graphite rod to obtain high-quality graphene composite material. The polymer or biomolecule is 1-ethoxy-3-methylimidazole sodium polystyrene benzene sulfonate, polyvinyl pyrrolidone, beta -cyclodextrin, chitosan, DNA, RNA, polypeptide, or protein. The electrolytic additive is acid, alkali, salt, or surfactant.