• 专利标题:   Preparing modified graphene oxide by taking graphene oxide for modification, preparing dispersion of graphene oxide, dispersing, weighing graphene oxide dispersion, placing in reactor and stirring, heating in water bath, dripping vinyltriethoxysilane, continuing to react, and leaving still.
  • 专利号:   CN113233449-A
  • 发明人:   LIU Y, WU J, LUO S, WANG K
  • 专利权人:   SHENZHEN GANGCHUANG BUILDING MATERIAL CO
  • 国际专利分类:   C01B032/194, C04B024/24
  • 专利详细信息:   CN113233449-A 10 Aug 2021 C01B-032/194 202177 Pages: 5 Chinese
  • 申请详细信息:   CN113233449-A CN10543888 19 May 2021
  • 优先权号:   CN10543888

▎ 摘  要

NOVELTY - Method for preparing modified graphene oxide involves (i) taking an appropriate amount of graphene oxide for modification, preparing a dispersion of 2 g/l graphene oxide, and dispersing under ultrasonic conditions for 2 hours, (ii) weighing 1000 g graphene oxide dispersion, placing in the reactor and stirring, and heating at 70 degrees C in a water bath, (iii) weighing 4 g vinyltriethoxysilane and adding to a reaction kettle by dripping for 0.5 hour, and (iv) continuing to react for 0.5 hours after the dripping, leaving still to cool down, and ending the test. USE - Method useful for preparing modified graphene oxide for preparing slump-preserving mother liquor (claimed). ADVANTAGE - The method participates in the synthesis of slump-preserving polycarboxylic acid mother liquor, effectively weakens the viscosity-increasing effect of graphene oxide on concrete, increases the utilization rate of graphene oxide, and ensures the slump retention performance of graphene-modified concrete over a period of time. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a formulation for preparing slump-preserving mother liquor using modified graphene oxide, comprising 300 g polycarboxylic acid macromonomer, 240 g modified graphene oxide dispersion, 2.75 g hydrogen peroxide, 69 g liquid (A), 112.4 g liquid (B), 35 g neutralization liquid and 160 g water, (or) 300 g polycarboxylic acid macromonomer, 240 g modified graphene oxide dispersion, 2.75 g hydrogen peroxide, 80 g solution (A), 103.5 g solution (B), 35 g neutralization solution and 240 g water.