▎ 摘　　要

NOVELTY - Preparing conductive polymer/graphene oxide composite material involves dissolving ferric chloride in a graphene oxide aqueous solution and dispersing ultrasonically to obtain a mixed ferric chloride/graphene oxide aqueous solution, putting aniline monomer and pyrrole monomer in different containers, and placing together in the same closed space with the ferric chloride/graphene oxide mixed aqueous solution. The air in the closed space is evacuated to form a vacuum, and a gas/liquid interface synthesis is performed to obtain a conductive polymer/graphene oxide composite material having a three-dimensional structure. USE - Method for preparing conductive polymer/graphene oxide composite material. ADVANTAGE - The method enables to prepare conductive polymer/graphene oxide composite material, where operation is convenient and safe, realizes industrialized mass production, and has good application prospects.