• 专利标题:   Method for preparing supported noble metal compound, involves heating obtained solid powder precursor in reducing atmosphere to reduce noble metal salt to obtain noble metal simple substance and obtain intermediate product, and reacting obtained intermediate product with the gas.
  • 专利号:   CN114182283-A, CN114182283-B
  • 发明人:   ZHANG J, SONG M, WANG D
  • 专利权人:   UNIV HUAZHONG SCI TECHNOLOGY
  • 国际专利分类:   C25B001/30, C25B011/054, C25B011/065, C25B011/075
  • 专利详细信息:   CN114182283-A 15 Mar 2022 C25B-011/065 202283 Chinese
  • 申请详细信息:   CN114182283-A CN11432741 29 Nov 2021
  • 优先权号:   CN11432741

▎ 摘  要

NOVELTY - The method involves dispersing noble metal salt and a carbon carrier into water, and heating to evaporate a solvent to dryness so that the noble metal salt is adsorbed on the carbon carrier to obtain a solid powder precursor. The obtained solid powder precursor is heated in a reducing atmosphere to reduce noble metal salt to obtain a noble metal simple substance and obtain an intermediate product. The obtained intermediate product is reacted with the gas obtained after the elemental chalcogen nonmetal sublimes in a reducing atmosphere, or the obtained intermediate product is directly placed in an oxygen-containing atmosphere for reaction at the temperature of 250-450 ℃ to obtain the carbon-supported noble metal compound. The noble metal element in the solid powder precursor is present in an amount of 5 to 40% by mass. USE - Method for preparing supported noble metal compound for cathodic oxygen reduction catalyst in process of preparing hydrogen peroxide by oxygen reduction (all claimed). Can also be used for chemical synthesis, pulp bleaching, environmental treatment and hydrogen peroxide fuel cells. ADVANTAGE - The method prepares the supported noble metal compound catalyst by simple low temperature method, improves the oxygen reduction reaction synthesis of hydrogen peroxide selectivity and activity, mild reaction condition, simple operation, and suitable for large-scale production. DESCRIPTION OF DRAWING(S) - The drawing shows a graphical representation of stability curve of the electrosynthesis hydrogen peroxide of the carbon-loaded platinum diselenide. (Drawing includes non-English language text).