• 专利标题:   Preparing fluorine-doped titanium dioxide(B)/reduced graphene oxide composite material useful for lithium battery cathode, comprises adding graphene oxide into acetic acid solution, adding e.g. glycolic acid, separating grey precipitate by anhydrous ethanol and water and calcining.
  • 专利号:   CN115548311-A
  • 发明人:   ZHOU Z, WEI M, LI Y
  • 专利权人:   UNIV FUZHOU
  • 国际专利分类:   H01M010/0525, H01M004/131, H01M004/36, H01M004/38, H01M004/485
  • 专利详细信息:   CN115548311-A 30 Dec 2022 H01M-004/36 202315 Chinese
  • 申请详细信息:   CN115548311-A CN11282983 20 Oct 2022
  • 优先权号:   CN11282983

▎ 摘  要

NOVELTY - Preparing fluorine-doped titanium dioxide(B)/reduced graphene oxide composite material, comprises (i) adding graphene oxide into the acetic acid solution, stirring uniformly, adding glycolic acid, tetrabutyl titanate and ammonium fluoride, stirring uniformly, transferring into a reaction vessel to react, separating the obtained grey precipitate by anhydrous ethanol and water, washing and centrifuging and drying, and (ii) drying the grey precipitate at 400℃ with a heating rate of 2℃/minute, calcining for 2 hours under nitrogen atmosphere. USE - The composite material is useful for lithium battery cathode (claimed). ADVANTAGE - The material has very high specific capacity and cycle stability, stable capacity at 202.3 mAh/g and exhibits excellent rate discharge performance. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are also included for: Fluorine-doped titanium dioxide(B)/reduced graphene oxide composite material prepared by above method; and Use of fluorine-doped titanium dioxide (B)/reduced graphene oxide composite material for lithium battery cathode.