• 专利标题:   Preparing graphene used for preparing titanium dioxide-graphene nano-composite material, by reducing dispersive graphite oxide in inert solvent to form graphene-containing reaction mixture, and isolating graphene from reaction mixture.
  • 专利号:   CN102976314-A, CN102976314-B
  • 发明人:   YU J, CHEN T, XIAO P
  • 专利权人:   CHINESE ACAD SCI NINGBO INST MATERIAL TE, CHINESE ACAD SCI NINGBO MATERIAL TECHNOL
  • 国际专利分类:   B01J021/18, C01B031/04, C01G023/053
  • 专利详细信息:   CN102976314-A 20 Mar 2013 C01B-031/04 201358 Pages: 12 Chinese
  • 申请详细信息:   CN102976314-A CN10506486 29 Nov 2012
  • 优先权号:   CN10506486

▎ 摘  要

NOVELTY - Preparing graphene comprises reducing dispersive graphite oxide in an inert solvent using a reducing agent to form a graphene-containing reaction mixture, and isolating graphene from the reaction mixture, where the reducing agent comprises sodium borohydride or vitamin C. USE - The method is useful for preparing graphene that is useful for preparing titanium dioxide-graphene nano-composite material (all claimed). ADVANTAGE - The titanium dioxide-graphene nano-composite material has efficient photocatalytic performance. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for: (1) performing surface modification of graphite alkene comprises dispersing the graphene into the solvent to form the graphene oxide solution and adding a modifying agent and the graphene with the graphene oxide solution under the ultrasonic wave in a surface modifier, where the modifier comprises pyrene, naphthalene or naphthalene derivatives; (2) preparing graphene nano-composite material using titanium dioxide comprising making a graphene-containing alcohol solution with surface modified titanium containing compounds, and preparing titanium dioxide-graphite nano composite material, where the composite material is provided with a set of titanium dioxide-graphene composite nano-particle each nanoparticles comprise surface modified graphene dispersedly located on surface of graphite alkene titanium dioxide particles and the composite material contains 5-20 wt.% of graphene based on the total weight of composite material; and (3) titanium dioxide-graphite nano-composite material.