• 专利标题:   Preparation of nano lithium iron phosphate/graphene composite material used for preparing lithium ion battery anode material includes dissolving iron sulfide in ethylene glycol, mixing, reacting, cooling, precipitating and drying.
  • 专利号:   CN107180965-A
  • 发明人:   WENG Y, WU Y, XIE J
  • 专利权人:   ZHEJIANG MEIDU GRAPHENE TECHNOLOGY CO
  • 国际专利分类:   B82Y030/00, H01M010/0525, H01M004/36, H01M004/58, H01M004/62
  • 专利详细信息:   CN107180965-A 19 Sep 2017 H01M-004/36 201774 Pages: 9 Chinese
  • 申请详细信息:   CN107180965-A CN10557551 10 Jul 2017
  • 优先权号:   CN10557551

▎ 摘  要

NOVELTY - Preparation of nano lithium iron phosphate/graphene composite material comprises preparing 0.3-3 mol/L lithium hydroxide/ethylene glycol solution and 0.2-2 mol/L phosphoric acid/ethylene glycol solution, dissolving iron sulfide in ethylene glycol, mixing, reacting at 150-200 degrees C for 5-15 hours, cooling, precipitating, centrifuging, drying, adding lithium iron phosphate and graphite oxide in water, mixing, adding hydrazine hydrate, placing in water bath at 70-90 degrees C for 3-10 hours, centrifuging and drying. USE - Method of preparing nano lithium iron phosphate/graphene composite material used for preparing lithium ion battery anode material (claimed). ADVANTAGE - The method is simple, has excellent large-current cycle stability, low energy consumption and low cost.