• 专利标题:   Preparing air purifying material comprises soaking hydrogel of bacterial cellulose in deionized water, compacting, electrostatic spinning, performing hydrothermal reaction, adding tetrabutyl titanate, and manganese chloride, and heating.
  • 专利号:   CN112538190-A, CN112538190-B
  • 发明人:   GAO Q
  • 专利权人:   YISHUI HONGYU ENVIRONMENTAL TECHNOLOGY, MO J
  • 国际专利分类:   B01D053/02, B01D053/56, B01D053/72, B01D053/86, C08J009/28, C08J009/40, C08K003/04, C08K003/22, C08L001/02, C08L033/20
  • 专利详细信息:   CN112538190-A 23 Mar 2021 C08J-009/40 202132 Pages: 5 Chinese
  • 申请详细信息:   CN112538190-A CN11272892 13 Nov 2020
  • 优先权号:   CN11272892

▎ 摘  要

NOVELTY - Preparing air purifying material comprises soaking hydrogel of bacterial cellulose in deionized water, compacting for removing water, heating and dissolving polyacrylonitrile, performing electrostatic spinning to obtain polyacrylonitrile nanofibers, and dispersing in solvent, dispersing graphene oxide in deionized water, adding bacterial cellulose and polyacrylonitrile nanofibers, stirring, then transferring to hydrothermal stirred tank for performing hydrothermal reaction, and freeze-drying to obtain graphene-polyacrylonitrile-bacterial cellulose aerogel, adding graphene-polyacrylonitrile-bacterial cellulose aerogel to deionized water, stirring, continuing adding tetrabutyl titanate, manganese chloride and potassium permanganate solution, mixing, adding ammonia solution in a drop wise manner, and heating to obtain graphene-polyacrylonitrile-bacterial cellulose aerogel-chromium doped titanium dioxide-manganese oxide composite material. USE - The method is useful for preparing air purifying material. DETAILED DESCRIPTION - Preparing air purifying material comprises (a) soaking hydrogel of bacterial cellulose in deionized water, and compacting for removing water, (b) heating and dissolving polyacrylonitrile, performing electrostatic spinning to obtain polyacrylonitrile nanofibers, and dispersing in solvent, (c) dispersing graphene oxide ultrasonically in deionized water, then adding bacterial cellulose and polyacrylonitrile nanofibers, stirring, then transferring to hydrothermal stirred tank for performing hydrothermal reaction, and freeze-drying to obtain graphene-polyacrylonitrile-bacterial cellulose aerogel, and (d) adding graphene-polyacrylonitrile-bacterial cellulose aerogel to deionized water, then adding chromium source, stirring, continuing adding tetrabutyl titanate, manganese chloride and potassium permanganate solution, mixing, adding ammonia solution in a drop wise manner, and heating at 140-200 degrees C for reacting for 5-10 hours to obtain graphene-polyacrylonitrile-bacterial cellulose aerogel-chromium doped titanium dioxide-manganese oxide composite material. An INDEPENDENT CLAIM is also included for air purifying material prepared by the above method.