• 专利标题:   Preparation of graphene oxide film crosslinked by borate involves hydrolyzing polyacrylonitrile base film, modifying, immersing base film in polyethyleneimine solution and immersing in graphene oxide and borate solution.
  • 专利号:   CN110559891-A
  • 发明人:   YAN X, TAO W, LI J, CHENG S, ZHANG Y, SUN Y
  • 专利权人:   UNIV HOHAI
  • 国际专利分类:   B01D067/00, B01D069/02, B01D069/12, B01D071/02, B01D071/82
  • 专利详细信息:   CN110559891-A 13 Dec 2019 B01D-071/82 202002 Pages: 7 Chinese
  • 申请详细信息:   CN110559891-A CN10886496 19 Sep 2019
  • 优先权号:   CN10886496

▎ 摘  要

NOVELTY - Preparation of graphene oxide film crosslinked by borate involves hydrolyzing polyacrylonitrile base film and modifying by an alkali solution, washing, drying, immersing modified base film in polyethyleneimine solution, drying, immersing base film containing polyethyleneimine in ultrasonically dispersed graphene oxide solution, cleaning, and drying, immersing base film containing graphene oxide in borate solution and directly drying and controlling number of repetitions of immersion in graphene oxide solution and borate solution. USE - Preparation of graphene oxide film. ADVANTAGE - The method provides graphene oxide film by simple process under mild reaction conditions, and uses borate as crosslinking agent to improve tensile strength and elastic modulus of graphene oxide film, and is environmentally- friendly.