• 专利标题:   Preparation of tin oxide-titanium oxide ternary graphene composite nanomaterial by adding deionized water and alcohol mixed solution to oxidized graphene, and adding hexadecyl trimethyl ammonium bromide and concentrated hydrochloric acid.
  • 专利号:   CN105529441-A, CN105529441-B
  • 发明人:   ZHANG H, GAO R, LI L, WANG Y, XU L
  • 专利权人:   UNIV SHANGHAI, UNIV SHANGHAI
  • 国际专利分类:   B82Y030/00, H01M004/36, H01M004/485
  • 专利详细信息:   CN105529441-A 27 Apr 2016 H01M-004/36 201644 Pages: 8 English
  • 申请详细信息:   CN105529441-A CN10589677 17 Sep 2015
  • 优先权号:   CN10589677

▎ 摘  要

NOVELTY - A tin oxide-titanium oxide ternary graphene composite nanomaterial is prepared by adding deionized water and alcohol mixed solution to oxidized graphene at a volume ratio of 2:1 to obtain a graphene solution having a concentration of 0.7 mol/l, adding hexadecyl trimethyl ammonium bromide and concentrated hydrochloric acid, stirring continuously for 0.5-1 hour, adding stannous chloride and titanyl sulfate, stirring continuously for 0.5-1 hour, heating at 120-180 degrees C for 12-24 hours, washing with deionized water, washing with ethyl alcohol, washing with deionized water, and drying. USE - Method of preparing tin oxide-titanium oxide ternary graphene composite nanomaterial. ADVANTAGE - The method is simple. DETAILED DESCRIPTION - A tin oxide-titanium oxide ternary graphene composite nanomaterial is prepared by adding deionized water and alcohol mixed solution to oxidized graphene at a volume ratio of 2:1 to obtain a graphene solution having a concentration of 0.7 mol/l, adding hexadecyl trimethyl ammonium bromide and concentrated hydrochloric acid, stirring continuously for 0.5-1 hour, adding stannous chloride and titanyl sulfate, stirring continuously for 0.5-1 hour, heating at 120-180 degrees C for 12-24 hours, washing with deionized water, washing with ethyl alcohol, washing with deionized water, and drying. The oxidized graphene, hexadecyl trimethyl ammonium bromide, concentrated hydrochloric acid, stannous chloride and titanyl sulfate have a mol ratio of 4.2:65:0.2:0.3.