• 专利标题:   Preparation of arched graphene three-dimensional network, involves taking three-dimensional copper mesh template, and using nickel-vapor-assisted graphene three-dimensional network gas phase chemical deposition growth method for growing.
  • 专利号:   CN106904601-A, CN106904601-B
  • 发明人:   ZHOU J, GUO C, CHEN Y, GUO W
  • 专利权人:   UNIV NANJING AERONAUTICS ASTRONAUTICS, UNIV NANJING AERONAUTICS ASTRONAUTICS
  • 国际专利分类:   C01B032/186, C01B032/194
  • 专利详细信息:   CN106904601-A 30 Jun 2017 C01B-032/186 201762 Pages: 19 Chinese
  • 申请详细信息:   CN106904601-A CN10119786 02 Mar 2017
  • 优先权号:   CN10119786

▎ 摘  要

NOVELTY - Preparation of arched graphene three-dimensional network, involves taking three-dimensional copper mesh as template, and using nickel-vapor-assisted graphene three-dimensional network gas phase chemical deposition growth method for growing, then cooling to room temperature, and obtaining three-dimensional network of graphene grown on three-dimensional copper network template, (ii) placing the three-dimensional network of graphene on a surface of semi-cured soft gel, performing natural settlement, and obtaining three-dimensional network of graphene semi-wrapped copper-containing core. USE - Preparation of arched graphene three-dimensional network (claimed). ADVANTAGE - The three-dimensional network of graphene grown on the three-dimensional copper-catalyzed template has excellent self-supporting property and optimal electrical transport performance for strain sensing. DETAILED DESCRIPTION - Preparation of arched graphene three-dimensional network, involves (i) taking three-dimensional copper mesh as a template, and using nickel-vapor-assisted graphene three-dimensional network gas phase chemical deposition growth method for growing for 30-60 minutes under the conditions of temperature of 990-1020 degrees C, methane flow rate of 20-50 sccm and hydrogen flow rate of 5-15 sccm, then cooling to room temperature, and obtaining three-dimensional network of graphene grown on three-dimensional copper network template, (ii) placing the three-dimensional network of graphene on a surface of semi-cured soft gel, performing natural settlement for 5-8 minutes, and obtaining three-dimensional network of graphene semi-wrapped copper-containing core, (iii) removing the copper core in the graphene three-dimensional network by continuously injecting an etching liquid, (iv) cleaning after removing the copper core from graphene three-dimensional network, and drying to obtain arched graphene three-dimensional network.