• 专利标题:   Preparation of degradable graphene composite electrospun fiber membrane involves dissolving polybutylene carbonate, polylactic acid and graphene in solvent, adding modified component to mixture, heating and electrospinning solution.
  • 专利号:   CN106702598-A
  • 发明人:   CHENG W, REN Z, GU X, WU Z, JIA H
  • 专利权人:   UNIV QIQIHAR
  • 国际专利分类:   D04H001/4382, D04H001/728
  • 专利详细信息:   CN106702598-A 24 May 2017 D04H-001/728 201748 Pages: 19 Chinese
  • 申请详细信息:   CN106702598-A CN10046956 22 Jan 2017
  • 优先权号:   CN10046956

▎ 摘  要

NOVELTY - Polybutylene carbonate, polylactic acid and graphene are dissolved in solvent. A modified component is added to mixture and stirred, to obtain electrospinning liquid. The electrospinning solution is heated at 50-60 degrees C for 2-4 hours and subjected to electrospinning at 50-60 degrees C, electrospinning voltage of 15-20 kV, spinning speed of 0.1-1.5 mL/hour and aluminum foil distance of 15-20 cm for 2-10 hours using spinning spinneret, to obtain degradable graphene composite electrospun fiber membrane. USE - Preparation of degradable graphene composite electrospun fiber membrane (claimed). ADVANTAGE - The method enables preparation of degradable graphene composite electrospun fiber membrane with excellent mechanical property. DETAILED DESCRIPTION - Polybutylene carbonate, polylactic acid and graphene are dissolved in solvent. A modified component is added to mixture and stirred at 320-640 rpm for 90-120 minutes, to obtain electrospinning liquid. The volume ratio of graphene and solvent is 0.005-0.04 g:10 mL. The mass ratio of graphene and polybutylene carbonate is 1:10-80. The mass ratio of graphene and polylactic acid is 1:50-400. The mass ratio of modified component and polybutylene carbonate is 0-5:100. The electrospinning solution is heated at 50-60 degrees C for 2-4 hours and subjected to electrospinning at 50-60 degrees C, electrospinning voltage of 15-20 kV, spinning speed of 0.1-1.5 mL/hour and aluminum foil distance of 15-20 cm for 2-10 hours using spinning spinneret, to obtain degradable graphene composite electrospun fiber membrane.