• 专利标题:   Preparation of graphene quantum dot involves calcining graphite, mixing with ammonium persulfate in N,N-dimethylformamide, ultrasonically dispersing, and hydrothermally reacting to obtain mixed solution containing graphene quantum dot.
  • 专利号:   CN109052381-A
  • 发明人:   YANG R, LIU R, XU D, MENG Q, LIU L, HUI P, CHEN L, YAN Y, XU Y, ZOU Y, DENG Q
  • 专利权人:   UNIV XIAN TECHNOLOGY
  • 国际专利分类:   C01B032/19
  • 专利详细信息:   CN109052381-A 21 Dec 2018 C01B-032/19 201908 Pages: 7 Chinese
  • 申请详细信息:   CN109052381-A CN11157734 30 Sep 2018
  • 优先权号:   CN11157734

▎ 摘  要

NOVELTY - The preparation of graphene quantum dot involves calcining graphite at high temperature, mixing graphite with ammonium persulfate in N,N-dimethylformamide to obtain mixed solution, stirring and ultrasonically dispersing, transferring the uniformly dispersed mixture to hydrothermal reaction kettle for reaction, cooling the product to room temperature, filtering carbon-based material through a porous filter to obtain a mixed solution containing graphene quantum dot, dialyzing the mixed solution containing graphene quantum dot in a dialysis bag to obtain graphene quantum dot aqueous solution and freeze-drying of graphene quantum dot aqueous solution. USE - Preparation of graphene quantum dot. ADVANTAGE - The method enables large-scale preparation of graphene quantum dot with uniform morphology and high yield.