• 专利标题:   Preparing graphene oxide foam loaded bismuth oxyiodide composite photocatalyst by impregnating graphene oxide dispersion, sintering, performing vacuum impregnation, soaking in solution comprising ethanol, taking sample, rinsing and drying.
  • 专利号:   CN110639561-A
  • 发明人:   HE R, JIA W, LIU H, GUI J, ZHOU J
  • 专利权人:   UNIV CHANGSHA
  • 国际专利分类:   B01J027/06, B01J035/02, C02F001/30, C02F101/30, C02F101/34
  • 专利详细信息:   CN110639561-A 03 Jan 2020 B01J-027/06 202008 Pages: 9 Chinese
  • 申请详细信息:   CN110639561-A CN10974432 14 Oct 2019
  • 优先权号:   CN10974432

▎ 摘  要

NOVELTY - Method for preparing graphene oxide foam loaded bismuth oxyiodide composite photocatalyst involves (i) taking a graphene oxide dispersion, impregnating with sponge, sintering, removing sponge to obtain graphene oxide foam with an interpenetrating network structure and carrying out vacuum impregnation on the graphene foam in a mixed solution of ethylene glycol, ethanol and water, so that the inner and outer surfaces of the graphene foam are wetted, (ii) preparing a mixed solution of bismuth nitrate and potassium iodide and (iii) soaking the graphene foam wetted in the step (i) into the mixed solution prepared in the step (ii), taking out a sample after a small amount of orange-red sediment exists on the graphene foam, sequentially carrying out rinsing several times using a mixed solution of ethylene glycol and water and using absolute ethyl alcohol and drying. USE - The method is useful for preparing the composite photocatalyst used as a photocatalyst for degradation of organic pollutants in water (claimed). ADVANTAGE - The method provides the composite photocatalyst with better exerting photocatalytic performance and a composite structure in which the graphene oxide foam does not block bismuth oxyiodide and does not affect the light absorption of bismuth oxyiodide. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for the composite photocatalyst prepared by the method.