• 专利标题:   Preparing hydroxyapatite/graphene nanocomposite, involves ultrasonically dispersing graphene in deionized water to obtain graphene dispersion, adding calcium nitrate to obtain mixed solution, and dripping aqueous ammonia.
  • 专利号:   CN104415399-A, CN104415399-B
  • 发明人:   HUANG J, LI H, LIU Y, YUAN J
  • 专利权人:   CHINESE ACAD SCI NINGBO INST MATERIAL, CHINESE ACAD SCI NINGBO MATERIALS TECHNOLOGY ENG INST
  • 国际专利分类:   A61K006/027, A61K006/033, A61L027/08, A61L027/12
  • 专利详细信息:   CN104415399-A 18 Mar 2015 A61L-027/12 201535 Pages: 13 Chinese
  • 申请详细信息:   CN104415399-A CN10409001 10 Sep 2013
  • 优先权号:   CN10409001

▎ 摘  要

NOVELTY - The method involves ultrasonically dispersing graphene in deionized water to obtain graphene dispersion, adding calcium nitrate to graphene dispersion and then stirring to obtain calcium nitrate/graphene mixed solution, dripping aqueous ammonia to mixed solution, dripping solution of calcium nitrate and diammonium phosphate and then reacting, stirring mixture to obtain hydroxyapatite/graphene precursor slurry, aging slurry to form composite material, washing, and drying and then grinding to obtain hydroxyapatite/graphene nanocomposite. USE - The method is useful for preparing hydroxyapatite/graphene nanocomposite (claimed). ADVANTAGE - The method is capable of preparing hydroxyapatite/graphene nanocomposite with improved mechanical and biological properties. DETAILED DESCRIPTION - The method involves ultrasonically dispersing graphene in deionized water to obtain a graphene dispersion having a concentration of 0.25-2.6 g/l, adding calcium nitrate to the graphene dispersion and then stirring to obtain calcium nitrate/graphene mixed solution, dripping aqueous ammonia to the mixed solution, adjusting pH value of the mixed solution to 11-14, dripping solution of calcium nitrate and diammonium phosphate to the mixed solution and then reacting, stirring the mixture to obtain hydroxyapatite/graphene precursor slurry, aging the slurry to form a composite material, washing, and drying and then grinding to obtain hydroxyapatite/graphene nanocomposite.