• 专利标题:   Preparation of graphene dispersion liquid by preprocessing graphite with organic solvent at high temperature, under inert gas protection, preprocessing graphite at high temperature, and ultrasonic peeling off graphite in solvent.
  • 专利号:   CN102659096-A
  • 发明人:   OU E, PENG H, XIE Y, XU W, XIONG Y, SONG Y
  • 专利权人:   UNIV HUNAN
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN102659096-A 12 Sep 2012 C01B-031/04 201323 Pages: 9 Chinese
  • 申请详细信息:   CN102659096-A CN10128930 27 Apr 2012
  • 优先权号:   CN10128930

▎ 摘  要

NOVELTY - Preparation of graphene dispersion liquid comprises preprocessing graphite with organic solvent at high temperature and at normal pressure or high pressure; under the protection of inert gas, preprocessing graphite at high temperature; ultrasonic peeling off graphite in a solvent; centrifuging; and separating to obtain graphene dispersion liquid. USE - Preparation of graphene dispersion liquid used for preparing graphene thin film (claimed). ADVANTAGE - The method provides high-quality and stable graphene dispersion liquid for preparing high-quality graphene film with controllable thickness; increases graphite interlayer distance to achieve ultrasonic peeling in a short period; uses simple device; and has mild condition and low cost. It solves the prior art problems of easy agglomeration and inability to realize industrial production. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparation of graphene thin film comprising taking graphene dispersion liquid or diluting to a certain concentration; transferring the diluted graphene dispersion liquid onto a substrate; and evaporating the solvent to obtain graphene film.