• 专利标题:   Preparation of composite fiber material involves immersing polyimide fiber in ethylenediamine solution and processing, adding graphene oxide and deionized water and drying, adding sodium borohydride and deionized water, and reacting.
  • 专利号:   CN106930100-A
  • 发明人:   ZHOU Z, WU X, BO W, ZHANG H, WANG Q
  • 专利权人:   UNIV SHANGHAI
  • 国际专利分类:   D06M101/30, D06M011/74, D06M013/332
  • 专利详细信息:   CN106930100-A 07 Jul 2017 D06M-011/74 201760 Pages: 7 Chinese
  • 申请详细信息:   CN106930100-A CN10166605 20 Mar 2017
  • 优先权号:   CN10166605

▎ 摘  要

NOVELTY - The preparation method of composite fiber material involves immersing 10-50 mg polyimide fiber in 10 ml ethylenediamine solution and then mixing, processing the mixture for 20 minutes to 1 hour and then washing using deionized water, adding 1-5 g graphene oxide and 4-20 ml deionized water to the mixture and then ultrasonically processing for 20-30 minutes, drying the mixture at 40-50 degrees C, adding 1.8-3.6 g sodium borohydride and 45-90 ml deionized water to the mixture and then reacting for 1-2 hours, adding deionized water to the mixture, and ultrasonically processing. USE - The method is useful for preparation of composite fiber material (claimed). ADVANTAGE - The method enables preparation of composite fiber material in simple and rapid manner. DETAILED DESCRIPTION - The preparation method of composite fiber material involves immersing 10-50 mg polyimide fiber in 10 ml ethylenediamine solution and then uniformly mixing, processing the mixture for 20 minutes to 1 hour and then washing using deionized water, adding 1-5 g graphene oxide and 4-20 ml deionized water to the mixture and then ultrasonically processing for 20-30 minutes, drying the mixture at 40-50 degrees C, adding 1.8-3.6 g sodium borohydride and 45-90 ml deionized water in a mass ratio of 1:(0.56-1.40) to the mixture and then reacting for 1-2 hours, adding deionized water to the mixture, and ultrasonically processing for 5-10 minutes.