• 专利标题:   Graphene oxide-reinforced denture base material is obtained by using raw material containing poly(methyl methacrylate) thermosetting denture base powder, base fluid, and graphite having preset purity.
  • 专利号:   CN108096037-A
  • 发明人:   LIU F
  • 专利权人:   LIU F
  • 国际专利分类:   A61K006/083, A61K006/027, A61K006/00
  • 专利详细信息:   CN108096037-A 01 Jun 2018 A61K-006/083 201857 Pages: 7 Chinese
  • 申请详细信息:   CN108096037-A CN11045060 24 Nov 2016
  • 优先权号:   CN11045060

▎ 摘  要

NOVELTY - Graphene oxide-reinforced denture base material is obtained by using a raw material containing poly(methyl methacrylate) thermosetting denture base powder, a base fluid, and graphite having purity of 99.9%. USE - Graphene oxide-reinforced denture base material. ADVANTAGE - The graphene oxide-reinforced denture base material has improved friction coefficient and wear rate based on the addition of graphene oxide, and excellent hydrophilicity and abrasion resistance. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for manufacture of graphene oxide-reinforced denture base material, which involves mixing high-purity natural graphite powder and anhydrous nitric acid with concentrated sulfuric acid in an ice bath, oxidizing the mixture with potassium permanganate as an oxidant, reducing excess oxidant with 30% hydrogen peroxide, filtering, washing, dehydrating to obtain graphene oxide, dissolving graphene oxide in deionized water, ultrasonically stirring at 500W for 30 minutes, adding 5 g pure poly(methyl methacrylate) dry powder, stirring for 1 hour, drying in an oven at 60 degrees C to remove deionized water, ball milling at rate of 400 rpm for 100 minutes to obtain graphene oxide/poly(methyl methacrylate)denture base mixed powder, mixing the denture base powder and water in volume ratio of 2:1, applying the mixture on a polyethylene film, pressing, heat-treating for 30 minutes in boiling water, naturally cooling to room temperature, and polishing the surface of the product.