• 专利标题:   Preparing graphene, comprises e.g. placing graphite into reactor, and then introducing reducing gas into reactor, heating and cooling reactor to obtain graphite powder, and adding powder to dimethylformamide or pentafluorophenyl nitrile.
  • 专利号:   CN102757035-A, CN102757035-B
  • 发明人:   WANG Y, ZHOU M, ZHONG L
  • 专利权人:   HAIYANGWANG LIGHTING TECHNOLOGY CO LTD, OCEANS KING LIGHTING SCI TECHNOLOGY CO, SHENZHEN OCEANS KING LIGHTING SCI TECH
  • 国际专利分类:   B82Y040/00, C01B031/04
  • 专利详细信息:   CN102757035-A 31 Oct 2012 C01B-031/04 201327 Pages: 7 Chinese
  • 申请详细信息:   CN102757035-A CN10105420 26 Apr 2011
  • 优先权号:   CN10105420

▎ 摘  要

NOVELTY - Preparing graphene, comprises placing (S1) a graphite into a reactor, and then introducing reducing gas into the reactor, heating and cooling the reactor at 800-1200 degrees C to obtain graphite powder, adding (S2) the powder to dimethylformamide or pentafluorophenyl nitrile, and then adding urea or ammonium acetate, performing ultrasonic dispersion to obtain a mixed solution, placing (S3) the mixed solution into a microwave reactor, adjusting the microwave power to 400-800 W, heating the mixed solution at 180-300 degrees C for 5-15 minutes, and filtering (S4), cleaning and drying the solution. USE - The method is useful for preparing graphene. ADVANTAGE - The method allows economical preparation of the graphene with high purity. DESCRIPTION OF DRAWING(S) - The figure shows a flow chart of a method for preparing graphene (Drawing includes non-English language text). Placing a graphite into a reactor (S1) Adding the graphite powder to dimethylformamide or pentafluorophenyl nitrile (S2) Placing the mixed solution into a microwave reactor (S3) Filtering, cleaning and drying the mixed solution. (S4)