• 专利标题:   Preparing multi-layer flame-retardant composite material involves dispersing N,N-dimethylformamide and graphene oxide, adding flame retardant, dispersing it and subjecting it to centrifugation and drying to obtain modified flame retardant I.
  • 专利号:   CN112940462-A
  • 发明人:   CHEN B, WANG Z, LI Z, ZHAO T, MAO J, LI J
  • 专利权人:   UNIV XIHUA
  • 国际专利分类:   C08K003/04, C08K005/29, C08L067/02, C08L091/06
  • 专利详细信息:   CN112940462-A 11 Jun 2021 C08L-067/02 202163 Pages: 12 Chinese
  • 申请详细信息:   CN112940462-A CN10122591 29 Jan 2021
  • 优先权号:   CN10122591

▎ 摘  要

NOVELTY - Preparing multi-layer flame-retardant composite material involves dispersing N,N-dimethylformamide and graphene oxide ultrasonically at 20-40 degrees C for 20-40 minutes, adding intumescent flame retardant, ultrasonically dispersing it at 20-40 degrees C for 20-40 minutes, and subjecting it to centrifugation, washing and drying to obtain modified flame retardant I. The N,N-dimethylformamide and graphene oxide are dispersed ultrasonically at 20-40 degrees C for 20-40 minutes, intumescent flame retardant is added and ultrasonically dispersed at 20-40 degrees C for 20-40 minutes, dicyclohexylcarbodiimide is added and mechanically stirred for 22-24 hours at 40-60 degrees C in water bath, and then centrifuged, cleaned and dried to obtain modified flame retardant II. The intumescent flame retardant and polybutylene terephthalate are dried at 70-90 degrees C for 8-12 hours, mixed in different mass ratios, modified flame retardant I and II, liquid paraffin and antioxidant are added at same time. USE - Method for preparing multi-layer flame-retardant composite material. ADVANTAGE - The method enables to prepare multi-layer flame-retardant composite material, which has simple and easy to control process, improves flame-retardant performance and mechanical property, and effectively solves problem that materials are easy to melt and drip and mechanical property is reduced. DETAILED DESCRIPTION - Preparing multi-layer flame-retardant composite material involves dispersing N,N-dimethylformamide and graphene oxide ultrasonically at 20-40 degrees C for 20-40 minutes, adding intumescent flame retardant, ultrasonically dispersing it at 20-40 degrees C for 20-40 minutes, and subjecting it to centrifugation, washing and drying to obtain modified flame retardant I. The N,N-dimethylformamide and graphene oxide are dispersed ultrasonically at 20-40 degrees C for 20-40 minutes, intumescent flame retardant is added and ultrasonically dispersed at 20-40 degrees C for 20-40 minutes, dicyclohexylcarbodiimide is added and mechanically stirred for 22-24 hours at 40-60 degrees C in water bath, and then centrifuged, cleaned and dried to obtain modified flame retardant II. The intumescent flame retardant and polybutylene terephthalate are dried at 70-90 degrees C for 8-12 hours, mixed in different mass ratios, modified flame retardant I and II, liquid paraffin and antioxidant are added at same time, extruded and granulated through a co-rotating twin-screw extruder, dried and subjected to injection molding to obtain final product.