• 专利标题:   Manufacture of graphene involves oxidizing natural graphite flake, ultrasonically-dispersing graphite oxide in acidic mother liquid, adjusting pH using aqueous ammonia, dehydrating, pre-reducing graphene oxide, heating, and reducing.
  • 专利号:   CN105347331-A, CN105347331-B
  • 发明人:   CAO Y, DU K, HU G, PENG Z, WU K
  • 专利权人:   UNIV CENT SOUTH
  • 国际专利分类:   C01B031/04, C01B032/19
  • 专利详细信息:   CN105347331-A 24 Feb 2016 C01B-031/04 201646 Pages: 6 English
  • 申请详细信息:   CN105347331-A CN10791140 17 Nov 2015
  • 优先权号:   CN10791140

▎ 摘  要

NOVELTY - Manufacture of graphene involves oxidizing natural graphite flake, ultrasonically-dispersing the obtained graphite oxide in acidic mother liquid to obtain acidic graphene dispersion liquid, adjusting pH to 6-7 by adding aqueous ammonia, dehydrating the graphene oxide dispersion liquid, pre-reducing graphene oxide, heating, drying and performing secondary reduction of dried graphene oxide at 500-800 degrees C under reducing atmosphere. USE - Manufacture of graphene (claimed). ADVANTAGE - The method is environmentally-friendly and safe, and enables efficient manufacture of graphene, by simple method.