• 专利标题:   Preparation of lithium iron phosphate used as anode material in power battery industry, by adding lithium and carbon sources to metal-doped lithium iron phosphate precursor prepared using ferric sulfate and phosphorus source, mixing, performing solid-phase reaction, and sintering.
  • 专利号:   CN114702021-A
  • 发明人:   ZENG N, YANG Y, SHI H, WANG W, WANG J, CHEN Y, XIE X, XU Y, HOU X, SHI B
  • 专利权人:   LANZHOU LS CAS NANO TECHNOLOGY CO LTD
  • 国际专利分类:   B82Y040/00, C01B025/45
  • 专利详细信息:   CN114702021-A 05 Jul 2022 C01B-025/45 202295 Chinese
  • 申请详细信息:   CN114702021-A CN10499493 09 May 2022
  • 优先权号:   CN10499493

▎ 摘  要

NOVELTY - Preparation of lithium iron phosphate involves: flowing a ferric sulfate solution, a phosphorus source, a dopant metal salt solution, and an additive into a multiphase reactor for liquid-phase precipitation to obtain a reaction slurry, aging the slurry, filtering, drying at 80-90°C for 18-20 hours, calcining at 500-700°C for 1.5-2.5 hours to obtain a metal-doped lithium iron phosphate precursor, adding a lithium source and a carbon source to the obtained product, mixing to obtain a lithium-doped iron phosphate solid mixture, subjecting the mixture to high-temperature solid-phase reaction at 600-850°C under inert gas protection, and sintering for 6-8 hours. USE - Preparation of lithium iron phosphate used as anode material in power battery industry. ADVANTAGE - The method provides lithium iron phosphate, which has high ion transmission efficiency, purity and stability, and ensures high production efficiency. The anode material has nano grain diameter.